✦ LIBER ✦

An efficient synthesis of [D6]leucocrystal violet

✍ Scribed by Weicheng Yang; Yong Luo; Weixia Liu; Xiaojun Deng; Xiaoning Du; Meihua Li

Publisher: John Wiley and Sons
Year: 2010
Tongue: French
Weight: 83 KB
Volume: 54
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.1849

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✦ Synopsis

Abstract

This report presents an efficient synthesis of [D~6~]leucocrystal violet. Esterification of p‐toluenesulphonyl chloride with [D~4~]methanol provided [D~3~]methyl p‐toluenesulphonate, which was used to methylate aniline to give [D~6~]N,N‐dimethylaniline. Condensation of [D~6~]N,N‐dimethylaniline with bis[4‐(dimethylamino)phenyl]methanol afforded [D~6~]leucocrystal violet in an overall yield of 30% in three steps. Copyright © 2010 John Wiley & Sons, Ltd.

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