Synthesis of phosphonic monoesters from phosphonous acids
β Scribed by Donald S Karanewsky; Michael C Badia
- Publisher
- Elsevier Science
- Year
- 1986
- Tongue
- French
- Weight
- 251 KB
- Volume
- 27
- Category
- Article
- ISSN
- 0040-4039
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β¦ Synopsis
Phosphonic monoesters are prepared in a two-step procedure by DCC-DMAP mediated esterification of phosphonous acids and oxidation of the resulting phosphonous monoester.
π SIMILAR VOLUMES
## Abstract For Abstract see ChemInform Abstract in Full Text.
## Abstract A series of phosphonic acid, 1,3,4βthiadiazolβ2βamineβ__N__βalkyl have been synthesized by the reaction of 2βamine thiadiazole, different aldehydes (or ketone), and phosphorous acid via the melting method or the solvent method. These compounds have been characterized by IR, ^1^H NMR, ^3