Synthesis of phosphonic acid containing thiadiazole

✍ Scribed by Hairong Hu; Chuanfang Zhu; Juan Fu

• Publisher: John Wiley and Sons
• Year: 2008
• Tongue: English
• Weight: 113 KB
• Volume: 19
• Category: Article
• ISSN: 1042-7163
• DOI: 10.1002/hc.20395

✦ Synopsis

Abstract

A series of phosphonic acid, 1,3,4‐thiadiazol‐2‐amine‐N‐alkyl have been synthesized by the reaction of 2‐amine thiadiazole, different aldehydes (or ketone), and phosphorous acid via the melting method or the solvent method. These compounds have been characterized by IR, ^1^H NMR, ^31^P NMR, and elemental analysis. Results showed that compounds were reacted via the solvent method in better yields. © 2008 Wiley Periodicals, Inc. Heteroatom Chem 19:140–143, 2008; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.20395