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Synthesis of new 1,3-thiazepine derivatives

✍ Scribed by Marta Struga; Jerzy Kossakowski; Barbara. Miroslaw; Anna E. Koziol; Andrzej Zimniak

Publisher: Journal of Heterocyclic Chemistry
Year: 2009
Tongue: English
Weight: 121 KB
Volume: 46
Category: Article
ISSN: 0022-152X
DOI: 10.1002/jhet.44

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✦ Synopsis

Abstract

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Condensation of thiourea derivatives with 1,4‐dibromobutane gave 1,3‐thiazepine derivatives (1a, 1b, 1c − 3a, 3b, 3c). Elementary analysis, MS and ^1^H NMR spectra confirmed the identity of the products. The molecular structure of 2b was determined by an X‐ray analysis. J. Heterocyclic Chem., (2009).

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