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Synthesis of (+)-goniothalamin and its enantiomer by combination of lipase catalyzed resolution and alkene metathesis

✍ Scribed by Eirik Sundby; Lars Perk; Thorleif Anthonsen; Arne Jørgen Aasen; Trond Vidar Hansen

Book ID
108282436
Publisher
Elsevier Science
Year
2004
Tongue
French
Weight
127 KB
Volume
60
Category
Article
ISSN
0040-4020

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Chemoenzymatic synthesis of duloxetine and its enantiomer: lipase-catalyzed resolution of 3-hydroxy-3-(2-thienyl) propanenitrile
✍ Ahmed Kamal; G.B.Ramesh Khanna; R Ramu; T Krishnaji 📂 Article 📅 2003 🏛 Elsevier Science 🌐 French ⚖ 157 KB

An efficient and facile chemoenzymatic synthesis of duloxetine by lipase mediated resolution of 3-hydroxy-3-(2thienyl)propanenitrile has been achieved. This process also describes an enantioconvergent synthesis of duloxetine via a Mitsunobu reaction.