Synthesis of cis- and trans-1,3,5,7-tetranitro-1,3,5,7-tetraazadecalin
✍ Scribed by Willer, Rodney L.
- Book ID
- 120519868
- Publisher
- American Chemical Society
- Year
- 1984
- Tongue
- English
- Weight
- 673 KB
- Volume
- 49
- Category
- Article
- ISSN
- 0022-3263
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📜 SIMILAR VOLUMES
The \({ }^{14} \mathrm{C}\)-uniformly labeled (UL) explosive, octahydro-1,3,5,7-tetranitro-1,3,5,7tetrazocine (HMX) was synthesized in \(40 \%\) yield by nitrolysis of \({ }^{14} \mathrm{C}\)-labeled hexamethylenetetramine (hexamine) in the presence of boron trifluoride diethyl etherate as catalyst.
## Abstract Procedures are described for the synthesis of 1,3,5‐trinitro‐1,3,5‐triazacyclohexane (RDX), 1,3,5,7‐tetranitro‐1,3,5,7‐tetraazacyclooctane (HMX) fully labeled with nitrogen‐15.
## Abstract A new series of relatively stable adducts of octahydro‐1,3,5,7‐tetranitro‐1,3,5,7‐tetrazocine (HMX) with derivatives of pyridine‐N‐oxide were prepared. In addition, relative stable new adducts of HMX were prepared with 5‐membered, 6‐membered, and condensed‐ring heterocyclic compounds. M