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Physico-Chemical Properties of 1,3,5,7-Tetranitro-1,3,5,7-Tetrazacyclooctane (HMX)

โœ Scribed by J. N. Maycock; V. R. Pai Verneker; W. Lochte

Publisher
John Wiley and Sons
Year
1969
Tongue
English
Weight
706 KB
Volume
35
Category
Article
ISSN
0370-1972

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New adducts of octahydro-1,3,5,7-tetrani
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## Abstract A new series of relatively stable adducts of octahydroโ€1,3,5,7โ€tetranitroโ€1,3,5,7โ€tetrazocine (HMX) with derivatives of pyridineโ€Nโ€oxide were prepared. In addition, relative stable new adducts of HMX were prepared with 5โ€membered, 6โ€membered, and condensedโ€ring heterocyclic compounds. M

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## Abstract Various methods of preparation of the different polymorphs of HMX have been evaluated. Infrared and Raman spectra have been used to differentiate the polymorphs and understand their conformational behaviour. Possible conformation of the ฮณ form has been suggested.

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The \({ }^{14} \mathrm{C}\)-uniformly labeled (UL) explosive, octahydro-1,3,5,7-tetranitro-1,3,5,7tetrazocine (HMX) was synthesized in \(40 \%\) yield by nitrolysis of \({ }^{14} \mathrm{C}\)-labeled hexamethylenetetramine (hexamine) in the presence of boron trifluoride diethyl etherate as catalyst.