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Potentiometric microdetermination of 1,3,5-trinitro-1,3,5-triazacyclohexane and 1,3,5,7-tetranitro-1,3,5,7-tetrazacyclooctane in several solvents

✍ Scribed by Walter Selig

Publisher
Elsevier Science
Year
1979
Tongue
English
Weight
354 KB
Volume
24
Category
Article
ISSN
0026-265X

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Synthesis of nitrogen-15 labeled 1,3,5-trinitro-1,3,5-triazacyclohexane (RDX) and 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane (HMX)
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## Abstract Procedures are described for the synthesis of 1,3,5‐trinitro‐1,3,5‐triazacyclohexane (RDX), 1,3,5,7‐tetranitro‐1,3,5,7‐tetraazacyclooctane (HMX) fully labeled with nitrogen‐15.

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## Abstract Relatively stable equimolar adducts of 1,3,5‐trinitro‐1,3,5‐triazacyclohexane were prepared with 2,6‐lutidine‐N‐oxide, 4‐hydroxy‐1‐butanesulfonic acid δ‐sultone (1,4‐butane sultone), and 2,2,6,6‐tetramethyl‐4‐piperidone‐1‐oxyl. Only the last adduct is selective for RDX; the others also

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## Abstract A new series of relatively stable adducts of octahydro‐1,3,5,7‐tetranitro‐1,3,5,7‐tetrazocine (HMX) with derivatives of pyridine‐N‐oxide were prepared. In addition, relative stable new adducts of HMX were prepared with 5‐membered, 6‐membered, and condensed‐ring heterocyclic compounds. M