Synthesis of [Carboxyl- 14 C]3,4-dehydro-DL-proline
โ Scribed by Hudson, CB; Robertson, AV
- Book ID
- 120809197
- Publisher
- Commonwealth Scientific and Industrial Research Organisation Publishing
- Year
- 1965
- Tongue
- English
- Weight
- 220 KB
- Volume
- 18
- Category
- Article
- ISSN
- 0004-9425
No coin nor oath required. For personal study only.
๐ SIMILAR VOLUMES
D L -t y r o ~i n e -4 -~~C has been synthesized with an overall yield 29.3 based on phenol-1-14C as the starting material. Anisole-l-14C was prepared by methylation of phenol-1-14C with dimethyl sulfate. The radioactive anisole was then converted to p-anisaldehyde-4-14C by a modijied Gattermann rea
## Abstract 2,3โDihydroxybenzoic acidโ(carboxylโ^14^C) can be synthesized in high overall yield from commerciallyโavailable 2,3โdimethoxybenzoic acid. The synthetic route features the application of a Curtius rearrangement, the thermal decomposition of a carboxylic acid azide to an isocyanate. The