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Synthesis of Biaryls via a Nickel(0)-Catalyzed Cross-Coupling Reaction of Chloroarenes with Arylboronic Acids

โœ Scribed by Saito, Syun; Oh-tani, Saori; Miyaura, Norio

Book ID
111877490
Publisher
American Chemical Society
Year
1997
Tongue
English
Weight
155 KB
Volume
62
Category
Article
ISSN
0022-3263

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ChemInform Abstract: Synthesis of Biaryl
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Synthesis of Biaryls via a Nickel(0)-Catalyzed Cross-Coupling Reaction of Chloroarenes with Arylboronic Acids. -Optimized conditions are found for coupling of a wide range of chloroarenes with various functionalized arylboronic acids using K 3 PO 4 as base and dioxane or benzene as solvent. Nickel(0

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The cross-coupling reaction of arylboronic acids (1.3 equivs) with aryl methanesulfonates was carded out in the presence of anickel(O) catalyst(3 tool%) and K3PO~,nH20 (3 equivs). The use of toluene as the solvent and the nickel(O)-dppf catalyst prepared from NiC~(dppf) plus dppf with BuLi were reco