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ChemInform Abstract: A Synthesis of Biaryls via Nickel(0)-Catalyzed Cross-Coupling Reaction of Chloroarenes with Phenylboronic Acids.

โœ Scribed by S. SAITO; M. SAKAI; N. MIYAURA

Book ID
112035628
Publisher
John Wiley and Sons
Year
2010
Weight
29 KB
Volume
27
Category
Article
ISSN
0931-7597

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Synthesis of Biaryls via a Nickel(0)-Catalyzed Cross-Coupling Reaction of Chloroarenes with Arylboronic Acids. -Optimized conditions are found for coupling of a wide range of chloroarenes with various functionalized arylboronic acids using K 3 PO 4 as base and dioxane or benzene as solvent. Nickel(0

Synthesis of biaryls via nickel-catalyze
Synthesis of biaryls via nickel-catalyzed cross-coupling reaction of arylboronic acids and aryl mesylates
โœ Masato Ueda; Atsushi Saitoh; Saori Oh-tani; Norio Miyaura ๐Ÿ“‚ Article ๐Ÿ“… 1998 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 407 KB

The cross-coupling reaction of arylboronic acids (1.3 equivs) with aryl methanesulfonates was carded out in the presence of anickel(O) catalyst(3 tool%) and K3PO~,nH20 (3 equivs). The use of toluene as the solvent and the nickel(O)-dppf catalyst prepared from NiC~(dppf) plus dppf with BuLi were reco