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Synthesis of 5α-pregnane-3β,20α-diol and of 5α-pregnane-3α,20α-diol labelled specifically at the 20β-position

✍ Scribed by T. A. Baillie; J. E. Herz; J. Sjövall

Publisher
John Wiley and Sons
Year
1974
Tongue
French
Weight
241 KB
Volume
10
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

A convenient synthesis of 5α‐[20β‐^2^H]pregnane‐3α,20α‐diol and 5α‐[20β‐^2^H]pregnane‐3β,20α‐diol from 3β‐hydroxy‐5α‐pregn‐16‐en‐20‐one is described. The reaction products are characterized by combined gas chromatography‐mass spectrometry.

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