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Synthesis of 4-OXO-5-aminopentanoic acid hydrochloride

โœ Scribed by S. I. Zav'yalov; A. G. Zavozin

Book ID
111930736
Publisher
Springer
Year
1987
Tongue
English
Weight
344 KB
Volume
36
Category
Article
ISSN
1573-9171

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A short synthesis of 5-amino[4-14]laevul
A short synthesis of 5-amino[4-14]laevulinic acid hydrochloride
โœ J B Cambell; J S Johnston ๐Ÿ“‚ Article ๐Ÿ“… 1989 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 219 KB

## 5-Amin0[4-'~C]laevulinic acid hydrochloride has been prepared from potassium [14C]cyanide in 56% overall yield. The key step is the palladium[O] catalysed coupling of 2-phthalimid0[l-'~C]acetyl chloride with 2-carboethoxyethylzinc iodide to give 5-phthalimid0[4-'~C]laevulinic acid ethyl ester i