Synthesis of 4-azido-2-isopropylamino-6-ethylamino-s-triazine (ring UL14C)
β Scribed by W.B. Burton
- Publisher
- Elsevier Science
- Year
- 1982
- Tongue
- English
- Weight
- 250 KB
- Volume
- 27
- Category
- Article
- ISSN
- 0026-265X
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π SIMILAR VOLUMES
## Abstract 2,4βDiaminoβ6β(diallylamino)β__s__βtriazineβ2,4β^14^C was prepared from K^14^CN in a four step sequence of reactions. The product was obtained in 26% yield at a specific activity of 1.01 mCi per mM. This product was converted to the hypotensive agent, 2,4βdiaminoβ6β(diallylamino)β__s__β
The s y n t h e s i s of t h e 5 -n i t r o f u r a n 2,4-diacetylamino-6-(5-nitro-2-furyl)- is d e s c r i b e d . F u r y l l i t h i u m i n e t h e r i s c a r b o x y l a t e d w i t h radio-carbon d i o x i d e g e n e r a t e d from Ba14COj. The furoic-carbonyl-14C a c i d is t h e n e s t e