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Synthesis of 3H- and 14C-labelled doisynolic and marrianolic acids, and stability of tritium label

✍ Scribed by Nakuleswar Kundu; Yoshio Osawa

Publisher
John Wiley and Sons
Year
1974
Tongue
French
Weight
231 KB
Volume
10
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

^3^H‐ and ^14^C‐Labelled doisynolic acid was prepared from 6,7‐^3^H‐, 2,4,6,7‐^3^H‐ and 4‐^14^C‐labelled oestradiol and oestrone by a regulated alkali fusion. Labelled marrianolic acid was similarly prepared from labelled oestriol. Unstability of regiospecific tritium labels in alkali was observed by use of double labelled compounds.

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