## Abstract For Abstract see ChemInform Abstract in Full Text.
Synthesis of 3′-azido-5′-homothymidine analogs
✍ Scribed by Claudie Gautier; Rolande Leroy; Claude Monneret; Pierre Roger
- Publisher
- Elsevier Science
- Year
- 1991
- Tongue
- French
- Weight
- 240 KB
- Volume
- 32
- Category
- Article
- ISSN
- 0040-4039
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
pectively (e.g. for (2a) in CC14: v, , (CSj) = 1146vw, vs(CS2) = 61 9 cm-1 vs). Spectroscopic and X-ray data indicate pseudooctahedral environment of the metal in (/a)--( 2f) with (pseudo)-Czv symmetry. The IH-NMR spectra indicate in particular that an isomeric mixture containing (Ze) and a tolyldit
S'-W]-3'-Azid~3'dcoxythymidinc @) was prepared at a specific activity of 14.0 Cilmmol by a twestep synthetic sequence involving controlled oxidation of the unlabelled compound c1) to the 5'-aldehyde (1) fdlowed by reduction with (W]-NaBH.. Purification was performed by preparative TLC. The radiochem