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Synthesis of 2,4′,5-trichloro [14C]biphenyl mercapturic acids

✍ Scribed by Ake Bergman; Jerome E. Bakke; Vernon J. Feil

Publisher
John Wiley and Sons
Year
1983
Tongue
French
Weight
286 KB
Volume
20
Category
Article
ISSN
0022-2135

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✦ Synopsis

The synthesis of 3-and 4-S-(N-acetyl)cysteinyl-2,4' ,5-tri~hloro?~CJbiphenyl is described. 4-ChloroC Claniline was used as starting material. The products were obtained after an aryl coupling of the amine with 2,5-dichloronitrobenzene, a reduction of the nitrogroup and finally coupling of the diazotized trichlorobiphenyl m i n e with cuprous N-acetylcysteine mercaptide.

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