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Synthesis of (±) [2-14C]mevalonolactone in one step

✍ Scribed by Asoke Banerji; Govind P. Kalena


Publisher
John Wiley and Sons
Year
1983
Tongue
French
Weight
136 KB
Volume
20
Category
Article
ISSN
0022-2135

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✦ Synopsis


Abstract

Condensation between 1‐trimethylsilyloxy‐3‐butanone and trimethylsilyl __[2‐^14^C]__acetate gave (±) [2‐^14^C]mevalonolactone in one step.


📜 SIMILAR VOLUMES


Synthesis of mevalonolactone-2,3-13C2
✍ Joseph I. Degraw; Ieaki Uemura 📂 Article 📅 1979 🏛 John Wiley and Sons 🌐 French ⚖ 115 KB

## Abstract The synthesis of mevalonolactone with ^13^C‐labels at positions 2 and 3 is reported. Hydrolysis of methyl 3‐hydroxy‐3‐methyl‐5,5‐dimethoxy‐valerate‐2,3‐^13^C~2~ to the aldehydo acid followed by reduction with sodium borohydride yielded the title compound. The material is useful as a sub

A simple, one-step synthesis of 1-14C-ac
✍ P. Mathiaparanam; L. T. Wong; B. H. Thomas 📂 Article 📅 1981 🏛 John Wiley and Sons 🌐 French ⚖ 220 KB

## Abstract A synthesis of 1‐^14^C‐acetylhydrazine by acetylation of hydrazine using 1‐ ^14^C‐ethyl acetate and a catalytic amount of activated alumina is described.

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✍ Lolita O. Zamir; Mubin Lin; Cong-Danh Nguyen 📂 Article 📅 1988 🏛 John Wiley and Sons 🌐 French ⚖ 217 KB

The chemical synthesis of double labelled mevalonolactone with carbon l a c at positions C-4 and C-6 is reported.

One step conversion of glutarimide-2,6-1
✍ L. H. McKendry 📂 Article 📅 1990 🏛 John Wiley and Sons 🌐 French ⚖ 208 KB 👁 1 views

## Abstract A convenient method of preparing 2‐octyl (4‐amino‐3,5‐dichloro‐6‐fluoro‐2‐pyridinyloxy‐2,6‐^14^C)acetate from glutarimide‐2,6‐^14^C is described. The process includes a novel one‐step conversion of glutarimide‐2,6‐^14^C to pentachloropyridine‐2,6‐^14^C.