𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Synthesis of [14C]propane

✍ Scribed by Desmond V. Dass; R. Wayne Martin; Allan L. Odell; Gregory Quinn

Publisher
John Wiley and Sons
Year
1988
Tongue
French
Weight
127 KB
Volume
25
Category
Article
ISSN
0022-2135

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

The synthesis of 14C-methylene diiodide
The synthesis of 14C-methylene diiodide and 14C-propane-1,3-dibromide
✍ A. R. Jones 📂 Article 📅 1975 🏛 John Wiley and Sons 🌐 French ⚖ 165 KB

## Abstract Existing methods have been adapted for the small scale synthesis of the title compounds in high yield. Modification of the iodoform reaction enables 1,3‐^14^C‐acetone (I) to be converted in over 95% yield to ^14^C‐iodoform (II) which is reduced by sodium aresenite to ^14^C‐methylene dii

Synthesis of 14C-labelled 1-(2,6-dimethy
Synthesis of 14C-labelled 1-(2,6-dimethyphenylamino)-2-dimethylamino-propane
✍ G. Zólyomi; Z. Zubovics; L. Toldy 📂 Article 📅 1983 🏛 John Wiley and Sons 🌐 French ⚖ 245 KB

The antiarrhytmic 1-(2,6-dimethylphenylamin0)-2--dimethylamino-propane (&) was labelled with I4C for pharmacokinetic study. A convenient synthesis, using 2-brom0propionyl-l-~~C chloride as radioactive key intermediate, involving an improved method for the reduction of N-( 2-dimethylaminopropionyl)-2

Synthesis of daunorubicin-14-14C and adr
Synthesis of daunorubicin-14-14C and adriamycin-14-14C
✍ C. Rolland Chen; Mary Tan Fon; Alan N. Fujiwara; David W. Henry; Morris A. Leaff 📂 Article 📅 1978 🏛 John Wiley and Sons 🌐 French ⚖ 275 KB

## Abstract Reaction of adriamycinone with excess ^14^CH~3~Mgl and periodate cleavage of the resulting glycol (5) affords daunomycinone‐14‐^14^C (6). Bromination and hydrolysis of 6 gives adriamycinone‐14‐^14^C (8). Coupling of 6 and the 14‐0‐p‐anisyldiphenyl‐methyl derivative (9) with 1‐chloro‐3‐N

Synthesis of 14-14C-adriamycin
Synthesis of 14-14C-adriamycin
✍ Babu R. Vishnuvajjala; Tadashi Kataoka; Frederick D. Cazer; Donald T. Witiak; Lo 📂 Article 📅 1978 🏛 John Wiley and Sons 🌐 French ⚖ 249 KB

14-14C-Adriamycin HC1 has been prepared from unlabeled adriamycin. The 14C-Diazald served as the source of the label. This synthesis does not require protection of the phenolic hydroxyl groups.

Synthesis of 14C-lanosterol and 14C-desm
Synthesis of 14C-lanosterol and 14C-desmosterol
✍ B. Danieli; G. Russo 📂 Article 📅 1965 🏛 John Wiley and Sons 🌐 French ⚖ 296 KB

The synthesis of lanosterol [la] and desmosterol [Ira] Iabeled with 14C in the 25 position by a Wittig reaction between triphenyl-214C isopropylidene-phosphorane [IVb] and the corresponding aldehydes are described. The specijic activities obtained are, respectively, 0.539 mClmM and 0.752 mClmM and t

Synthesis of 14C-labelled compounds. I.
Synthesis of 14C-labelled compounds. I. Synthesis of 2 (14C)-dinitrosohexahydropyrimidine
✍ Horst Brann; Barbara Bertram; Manfred Wiessler 📂 Article 📅 1977 🏛 John Wiley and Sons 🌐 French ⚖ 184 KB 👁 1 views

## Abstract A convenient procedure to synthesize 2–^14^C‐dinitroso‐hexahydropyrimidine (DNHP) is described. The synthesis begines with the condensation of ^14^C‐formaldehyde and propylenediamine‐1,3 in benzene with azeotropic removal of water. The resulting bases are isolated from the reaction mixt