## Abstract A scheme is developed for synthesizing ^14^C labelled α‐acetates of secondary α‐hydroxylated nitrosamines. In this manner ^14^C‐methyl (1‐acetoxy)ethyl nitrosamine and 1‐^14^C‐ethyl (1‐acetoxy)ethyl nitrosamine are synthesized in 16.3 and 33.3% yield, radiochemically pure.
Synthesis of 14C-methyl benzyl nitrosamine and methyl 14C-benzyl nitrosamine
✍ Scribed by Paul L. Skipper
- Publisher
- John Wiley and Sons
- Year
- 1978
- Tongue
- French
- Weight
- 201 KB
- Volume
- 15
- Category
- Article
- ISSN
- 0022-2135
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✦ Synopsis
The synthesis of k -l a b e l l e d methyl benzyl n i t r o s - amine is reported. Two fonns were prepared, one with a l a b e l i n the methyl group and one with l a b e l i n the methylene portion of t h e benzyl group. a c t i v i t i e s were approximately 5 mCi/mmol.
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