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Synthesis of 14C-labelled nitrosamines. IV synthesis of 14C-methyl-(1-acetoxy) methyl nitrosamine and 1-14C-ethyl (acetoxy)ethyl nitrosamine

✍ Scribed by Horst Braun; Manfred Wiessler

Publisher
John Wiley and Sons
Year
1978
Tongue
French
Weight
228 KB
Volume
14
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

A scheme is developed for synthesizing ^14^C labelled α‐acetates of secondary α‐hydroxylated nitrosamines. In this manner ^14^C‐methyl (1‐acetoxy)ethyl nitrosamine and 1‐^14^C‐ethyl (1‐acetoxy)ethyl nitrosamine are synthesized in 16.3 and 33.3% yield, radiochemically pure.

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