Synthesis of 13N-labelled amines by reduction of 13N-labelled amides
β Scribed by Toshiyoshi Tominaga; Osamu Inoue; Kazutoshi Suzuki; Toshio Yamasaki; Masaaki Hirobe
- Publisher
- Elsevier Science
- Year
- 1986
- Weight
- 293 KB
- Volume
- 37
- Category
- Article
- ISSN
- 0883-2889
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π SIMILAR VOLUMES
## Abstract A method for the production of ^13^NN either as a gas or as an injectable solution is described. The method is based on the ^16^O(p,Ξ±)^13^N reaction and water as target material. Following irradiation, the ^13^NO and ^13^NO are reduced to ^13^NH~3~, followed by NaOBr oxidation to ^13^NN
1 3 e n r i c h e d n -a l k y l c h l o r o s i l a n e s w i t h l a b e l i nc o r p o r a t i o n a t s e l e c t i v e p o s i t i o n s a l o n g t h e a l k y l c h a i n s . Compounds w h i c h w e r e p r e p a r e d w e r e : n -n o n y l t r i c h l o r o s i 1 a n e -1 -' 3 C n -d o d e
## Abstract The introduction of several ^13^Cβatoms in the alkane chain is described. A maximum number of compounds, with up to six ^13^C labels, are obtained with a minimum of different reactions.