For less labor-intensive, larger-scale, and more efficient production of D-[ 1-13C] glucose and other labeled monosaccharides using the cyanohydrin reduction reaction, an automated reactor was designed, constructed, and tested. A suitable vessel and all ancillary and control equipment were fabricate
Fully automated synthesis of 13N-labeled nitrosothiols
✍ Scribed by Vanessa Gómez-Vallejo; Koichi Kato; Iosu Oliden; Javier Calvo; Zuriñe Baz; José I. Borrell; Jordi Llop
- Publisher
- Elsevier Science
- Year
- 2010
- Tongue
- French
- Weight
- 595 KB
- Volume
- 51
- Category
- Article
- ISSN
- 0040-4039
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
1 3 e n r i c h e d n -a l k y l c h l o r o s i l a n e s w i t h l a b e l i nc o r p o r a t i o n a t s e l e c t i v e p o s i t i o n s a l o n g t h e a l k y l c h a i n s . Compounds w h i c h w e r e p r e p a r e d w e r e : n -n o n y l t r i c h l o r o s i 1 a n e -1 -' 3 C n -d o d e
## Abstract Anandamide (Figure 1a) (arachidonyl ethanolamide, AEA), (5Z,8Z,11Z,14Z)‐N‐(2‐hydroxyethyl)‐5,8,11,14‐Eicosatetraenamide, is an endogenous cannabinoid ligand possessing important biological activity. The conformation of AEA in its native receptor binding environment is particularly of in
## Abstract The synthesis of 1‐(2‐^13^C)‐cyclopropyl‐4‐phenyl‐1,2,3,6‐tetrahydropyridine (8) is reported. Attempts were first made to prepare labeled cyclopropylamine via a cyclopropanation/Curtius rearrangement sequence, but the yields were too modest to be suitable for the synthesis of a labeled