𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Synthesis of 13C-labelled cinnamonitrile

✍ Scribed by Elizabeth M. Zippi; Evan Kamperman


Publisher
John Wiley and Sons
Year
2002
Tongue
French
Weight
65 KB
Volume
45
Category
Article
ISSN
0022-2135

No coin nor oath required. For personal study only.

✦ Synopsis


Abstract

^13^C‐labelled cinnamonitrile, a compound that possesses both the aromatic functionality of styrene and the nitrile functionality of acrylonitrile has been synthesized in one step using β‐bromostyrene and potassium [^13^C]cyanide. The preparation of a target material using ^13^C ‐labelled cinnamonitrile may provide a cost‐effective method for producing nitrogen‐13 via proton irradiation for Positron Emission Tomography. Copyright © 2002 John Wiley & Sons, Ltd.


📜 SIMILAR VOLUMES


Synthesis of 13C-labelled tetramethyltet
✍ Jørn B. Christensen; Klaus Bechgaard; Gael Paquignon 📂 Article 📅 2001 🏛 John Wiley and Sons 🌐 French ⚖ 105 KB 👁 1 views

## Abstract The synthesis of tetramethyltetraselenafulvalene (4,4′,5,5′‐tetramethyl Δ^2,2′^‐bis‐1,3‐diselenole) doubly labelled with carbon‐13 in the 2 and 2′‐positions is described. Copyright © 2001 John Wiley & Sons, Ltd.

Synthesis of 13C- and 14C-labelled catec
✍ Rong Ji; Andreas Schäffer 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 French ⚖ 93 KB

## Abstract ^13^C‐ and ^14^C‐uniformly labelled catechol was synthesized from phenol in three steps. Phenol was derivatized with 2‐chloro‐5‐nitrobenzophenone in THF containing NaH, followed by __ortho__‐hydroxylation with 35% aqueous H~2~O~2~ in sulphuric acid/glacial acetic acid solution, and by c

Synthesis of 14C-labeled levamisole and
✍ V. J. Feil 📂 Article 📅 1996 🏛 John Wiley and Sons 🌐 French ⚖ 275 KB 👁 2 views

The syntheses of '%-ring labeled levamisole ([-)-2,3,5,6-tetrahydr0-6-phenyl[~'C-UL]imidazo(Z, 1b]thiole) from acetophenone-ring-UL-l'C in 5 steps plus resolution with a 7.5% overall yield, and %,-ring labeled tetramisole ([i]-2,3,5,6-tetrahydro-6-phenyif3 S ]imidaz0[2,?-bjthiazole) from benzene-'%,

Synthesis of 13C-enriched and 14C-labell
✍ Mohammad E. Mehrsheikh; Lane A. Clizbe; Harbhajan Singh; Wr Purdum 📂 Article 📅 1990 🏛 John Wiley and Sons 🌐 French ⚖ 314 KB

## Abstract This report describes the synthesis of the ^13^C‐enriched and ^14^C‐labelled title compound starting from isotopically labelled isovaleraldehyde.