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Synthesis of 1,3-Dimethylbicyclo[1.1.0]butane

✍ Scribed by Dr. K. Griesbaum; Dr. P. E. Butler

Publisher
John Wiley and Sons
Year
1967
Tongue
English
Weight
219 KB
Volume
6
Category
Article
ISSN
0044-8249

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✦ Synopsis

  1. Addition of Lip-thiocresolate gives a mixture of ( l ) , (Ia), ( l b ) , ( l c ) , i.e. p-tolylthio groups are incorporated into the carbenoid via (2) ; after a reaction time of 20 h at a temperature of -lOΒ°C the mixture was hydrolysed with D2O and H20 and the formation of the lithium compounds (1) through ( l c ) proved by NMR analysis of the hydrolysatesW

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