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Synthese des 1,3-Dimethyl-bicyclo[1.1.0]butans

✍ Scribed by Dr. K. Griesbaum; Dr. P. E. Butler

Publisher: John Wiley and Sons
Year: 1967
Tongue: English
Weight: 222 KB
Volume: 79
Category: Article
ISSN: 0044-8249
DOI: 10.1002/ange.19670791005

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2. Addition of Lip-thiocresolate gives a mixture of ( l ) , (Ia), ( l b ) , ( l c ) , i.e. p-tolylthio groups are incorporated into the carbenoid via (2) ; after a reaction time of 20 h at a temperature of -lO°C the mixture was hydrolysed with D2O and H20 and the formation of the lithium compounds (