Synthesis of 1,3-Dimethylbicyclo[1.1.0]b
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Dr. K. Griesbaum; Dr. P. E. Butler
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Article
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1967
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John Wiley and Sons
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English
โ 219 KB
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2. Addition of Lip-thiocresolate gives a mixture of ( l ) , (Ia), ( l b ) , ( l c ) , i.e. p-tolylthio groups are incorporated into the carbenoid via (2) ; after a reaction time of 20 h at a temperature of -lOยฐC the mixture was hydrolysed with D2O and H20 and the formation of the lithium compounds (