Synthesis and Molecular Structure of the
✍
Prof. Dr. Lothar Weber; Dipl.-Chem. Dagmar Bungardt; Uwe Sonnenberg; Dr. Roland
📂
Article
📅
1988
🏛
John Wiley and Sons
🌐
English
⚖ 389 KB
40°C. Slow warm-up to room temperature, column chromatographic work-up (silica gel flash chromatography, elution with a 10 : 1 : 1 mixture of dichloromethane, petroleum ether (30-50°C) and diethyl ether), and Kugelrohr distillation (bath temperature 45 "C at 0.1 torr) afforded the a-methylene-p-lact