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Synthesis and characterisation of sterically bulky lithium amidinate and bis-amidinate complexes

✍ Scribed by Robert J. Baker; Cameron Jones

Book ID
118475744
Publisher
Elsevier Science
Year
2006
Tongue
English
Weight
611 KB
Volume
691
Category
Article
ISSN
0022-328X

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The synthesis of novel bis(amidinate) silicon and germanium complexes is described. The reaction of two equiv. of [MeC(NiPr) 2 ]Li β€’ THF (1) with SiCl 4 , GeCl 4 or GeCl 2 β€’dioxane affords [MeC(NiPr) 2 ] 2 SiCl 2 (2), [MeC(NiPr) 2 ] 2 GeCl 2 (3) and