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Syntheses with stable isotopes: Sodium cyanide-13C

✍ Scribed by Thomas W. Whaley; Donald G. Ott

Publisher
John Wiley and Sons
Year
1975
Tongue
French
Weight
238 KB
Volume
11
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

Sodium cyanide‐ ^13^C has been prepared in 65–70% overall yield from carbon‐^13^C monoxide in a three‐step synthesis proceeding through isopropyl formate‐ ^13^C and formamide‐ ^13^C as intermediates. Several. methods for the dehydration of formamide have been investigated.

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