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Studies on isocyanides. Synthesis of N-tosylguanidines

โœ Scribed by Ricardo Bossio; Stefano Marcaccini; Roberto Pepino

Book ID
103403778
Publisher
Elsevier Science
Year
1995
Tongue
French
Weight
104 KB
Volume
36
Category
Article
ISSN
0040-4039

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## Abstract The Ugi fourโ€component condensation between isocyanides, aldehydes, and ammonium formate affords __N__โ€substituted 2โ€formylaminocarboxamides 1 which are dehydrated with POCl~3~/NEt~3~ to give the title compounds.

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Electrochemical Synthesis of Isocyanides and 1,n-Diisocyanides. -Electrolysis of tosylmethylisocyanides (I) and (III) gives the new alkyl-, aryl-, and 1,n-diisocyanides (II) and (IV) in high purity and in moderate to good yields. The reaction proceeds in a two-electron C,S cleavage, reducing exclusi