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Solid-Phase Synthesis of 1,2,3,4-Tetrahydro-2-pyridones via Aza-Annulation of Enamines

✍ Scribed by Paulvannan, K.; Chen, Tao


Book ID
127022641
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
97 KB
Volume
65
Category
Article
ISSN
0022-3263

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Synthesis of 4,6-Dimethyldibenzothiophen
✍ Xiaoying Xu; Xiang Li; Anjie Wang; Yinyong Sun; W. Bernd Schweizer; Roel Prins 📂 Article 📅 2011 🏛 John Wiley and Sons 🌐 German ⚖ 270 KB

## Abstract 1,2,3,4‐Tetrahydro‐4,6‐dimethyldibenzothiophene was prepared by coupling 2‐bromo‐3‐methylcyclohexanone with 2‐methylbenzenethiol and annulating the product with the aid of polyphosphoric acid. A mixture of 1,2,3,4‐tetrahydro‐4,6‐dimethyldibenzothiophene and 4,6‐dimethyldibenzothiophene