The title compound, C 9 H 12 BrNO 4 SÁH 2 O, was prepared by a reduced condensation reaction of 5-bromo-2-hydroxybenzaldehyde and 2-aminoethanesulfonic acid. In the crystal structure, a two-dimensional network is formed via intermolecular N-HÁ Á ÁO and O-HÁ Á ÁO hydrogen bonds.
Sodium 2-(N-morpholino)ethanesulfonate monohydrate
✍ Scribed by Deschamps, Jeffrey R. ;Flippen-Anderson, Judith L. ;George, Clifford
- Publisher
- International Union of Crystallography
- Year
- 2002
- Tongue
- English
- Weight
- 174 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
In the structure of caesium chloride 2-(N-morpholinio)ethanesulfonate, Cs + ÁCl À ÁC 6 H 13 NO 4 S, determined by X-ray diffraction analysis at 100 K, the caesium cation is coordinated by the chloride anion and six O atoms.
Starting from C1-14Cl ethanol 1 , 2-dibrom-C14C1ethane was prepared by an usual method through C14C3ethylene. Sodium sulfite was alkylated by 1,2-dibrom--C Clethane and the formed sodium 2-br0m-L~~Clethane sulfonate was transferred without isolation to a labelled 2-I: (aminoiminomethyl) thiol -C14C1
In the complex anion of the title compound, Na[Re(C~10~H~8~N~2~O~2~S~2~)O]·H~2~O, the Re atom adopts a square-pyramidal coordination, in which the Re=O bond is apical and the __S__,__N__,__N__,__S__-tetradentate ligand spans the four basal sites. The Na^+^ counter-ion is octahedrally surrounded by o