2-(5-Bromo-2-hydroxybenzylammonio)ethanesulfonate monohydrate
✍ Scribed by Xiao, Yu ;Gao, Shi-Xiang ;Sun, Cheng
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 273 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The title compound, C 9 H 12 BrNO 4 SÁH 2 O, was prepared by a reduced condensation reaction of 5-bromo-2-hydroxybenzaldehyde and 2-aminoethanesulfonic acid. In the crystal structure, a two-dimensional network is formed via intermolecular N-HÁ Á ÁO and O-HÁ Á ÁO hydrogen bonds.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 110 K Mean (C-C) = 0.004 A Disorder in solvent or counterion R factor = 0.036 wR factor = 0.106 Data-to-parameter ratio = 12.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The bond lengths in the title compound, C 13 H 11 N 3 O 2 ÁH 2 O indicate that the organic molecule exists in the keto form. A network of O-HÁ Á ÁO, O-HÁ Á ÁN and N-HÁ Á ÁO hydrogen bonds helps to consolidate the crystal packing.