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3-(5-Bromo-2-hydroxy­benzyl­ammonio)propanoate

✍ Scribed by Yin, Xiu-Ju ;Cai, Jin-Hua ;Ng, Seik Weng

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
117 KB
Volume
62
Category
Article
ISSN
1600-5368

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The title compound, C 9 H 12 BrNO 4 SÁH 2 O, was prepared by a reduced condensation reaction of 5-bromo-2-hydroxybenzaldehyde and 2-aminoethanesulfonic acid. In the crystal structure, a two-dimensional network is formed via intermolecular N-HÁ Á ÁO and O-HÁ Á ÁO hydrogen bonds.

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.011 A Ê R factor = 0.075 wR factor = 0.163 Data-to-parameter ratio = 13.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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N-(4-Bromobenzylidene)-2-hydroxyaniline, C 13 H 10 BrNO, exists as a planar molecule in which the hydroxy group is intramolecularly hydrogen bonded to the imino N atom.