𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Separation of histamine and its metabolites using glass capillary gas chromatography and a nitrogen detector

✍ Scribed by Lieu, Fong-Yi ;Jennings, W.


Publisher
John Wiley and Sons
Year
1980
Tongue
English
Weight
140 KB
Volume
3
Category
Article
ISSN
0935-6304

No coin nor oath required. For personal study only.

✦ Synopsis


Abstract

Complete separation of the TMS derivatives of histamine, 1‐methyl histamine and 3‐methyl histamine was achieved in two minutes in a 7 m Γ— 0.25 mm column coated with SP 2250. Using NPD, histamine was detectable at levels as low as 20 pg. This offers a rapid, sensitive procedure with potential for clinical diagnosis and food analysis.


πŸ“œ SIMILAR VOLUMES


Simultaneous determination of glyceryl t
✍ Langseth-Manrique, K. ;Bredesen, J. E. ;Greibrokk, T. πŸ“‚ Article πŸ“… 1986 πŸ› John Wiley and Sons 🌐 English βš– 442 KB πŸ‘ 2 views

A specific, sensitive, and precise assay for simultaneous quantitation of glyceryl trinitrate (GTN) and its metabolites 1,2and 1,3-glyceryl dinitrate (GDN) has been developed. The method involves one single extraction step with benzene, followed byevaporation at 55'C.One plof theextractwasinjected o

Gas-liquid chromatography of amino acids
✍ Moodie, I. M. ;Burger, J. πŸ“‚ Article πŸ“… 1981 πŸ› John Wiley and Sons 🌐 English βš– 423 KB πŸ‘ 1 views

## Abstract A carefully Standardized technique is described for the preparation of glass capillary columns which can be used successfully for routine quantitative amino acid analysis. Comparison is made between two different modes of sample injection. Preliminary quantitative results from β€œsplit” i

Rapid on-line analysis of low molecular
✍ Glajch, J. L. ;Schunn, R. A. πŸ“‚ Article πŸ“… 1981 πŸ› John Wiley and Sons 🌐 English βš– 324 KB πŸ‘ 1 views

## Abstract Rapid analysis is important for on‐line chromatography. Gaseous or vaporized samples have been injected via heated gas sampling valves of less than 500 ΞΌl dead volume. The critical sampling and split problems could be solved by temperature programming. The general analysis described cou

Highly sensitive determination of halope
✍ Nagai, Yumi ;Arimoto, Hiromi ;Fujii, Toshihiro πŸ“‚ Article πŸ“… 1990 πŸ› John Wiley and Sons 🌐 English βš– 270 KB πŸ‘ 1 views

## Abstract A method has been developed for highly sensitive determination of haloperidol in human serum involving a simple extraction procedure followed by gas chromatographic separation. Target components were separated from the extracting solvents with a Van den Berg type solventless sample inje