Sensitivity Enhancement and Heteronuclear Distance Measurements in Biological 17 O Solid-State NMR
β Scribed by Brinkmann, Andreas; Kentgens, Arno P. M.
- Book ID
- 127088788
- Publisher
- American Chemical Society
- Year
- 2006
- Tongue
- English
- Weight
- 281 KB
- Volume
- 110
- Category
- Article
- ISSN
- 0022-3654
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π SIMILAR VOLUMES
Free induction decay (FID) signals in solid state NMR measurements performed with magic angle spinning can often be extended in time by factors on the order of 10 by a simple pulsed spin locking technique. The sensitivity of a structural measurement in which the structural information is contained i
The initial results of optically-pumped, directly-detected NMR experiments on InP are reported. At low temperatures (4.2 K and above) and in a 9.39 T magnetic field, irradiation of a sample of an undoped InP wafer with 835-nm-wavelength light from a diode laser enhances the spin polarization of 31P
## Abstract Rotational resonance (R^2^) and rotational echo double resonance (REDOR) are powerful solidβstate NMR techniques that can be applied in a siteβdirected fashion for precise distance measurements in proteins. These tools are well suited for systems in which a few precise distance measurem