Nuclear Distance Measurements in Solid State NMR Spectroscopy
β Scribed by Shimon Vega
- Publisher
- John Wiley and Sons
- Year
- 2005
- Weight
- 8 KB
- Volume
- 36
- Category
- Article
- ISSN
- 0931-7597
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π SIMILAR VOLUMES
The accuracy with which distances can be measured using dipolar recoupling experiments in solid-state NMR is investigated. The relative precision of experiments in a three spin system versus an isolated spin pair is found to depend very strongly on the nature of the coupling Hamiltonian. The accurac
## Abstract Rotational resonance (R^2^) and rotational echo double resonance (REDOR) are powerful solidβstate NMR techniques that can be applied in a siteβdirected fashion for precise distance measurements in proteins. These tools are well suited for systems in which a few precise distance measurem