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Measurement of heteronuclear bond distances in polycrystalline solids by solid-state NMR techniques

โœ Scribed by Roberts, James E.; Harbison, Gerard S.; Munowitz, Michael G.; Herzfeld, Judith; Griffin, Robert G.

Book ID
111965759
Publisher
American Chemical Society
Year
1987
Tongue
English
Weight
941 KB
Volume
109
Category
Article
ISSN
0002-7863

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The accuracy with which distances can be measured using dipolar recoupling experiments in solid-state NMR is investigated. The relative precision of experiments in a three spin system versus an isolated spin pair is found to depend very strongly on the nature of the coupling Hamiltonian. The accurac