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Distance Measurements by Dipolar Recoupling Two-Dimensional Solid-State NMR

โœ Scribed by Kiihne, S.; Mehta, M. A.; Stringer, J. A.; Gregory, D. M.; Shiels, J. C.; Drobny, G. P.


Book ID
126193373
Publisher
American Chemical Society
Year
1998
Tongue
English
Weight
454 KB
Volume
102
Category
Article
ISSN
1089-5639

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A series of uni-and multidimensional variants of the dipolar exchange-assisted recoupling (DEAR) NMR experiment is described and applied to determinations of 13 C-14 N dipolar local field spectra in amino acids and dipeptides. The DEAR protocol recouples nearby nuclei by relying on differences in th