Two techniques for resolution and sensitivity enhancement are introduced in multiple-quantum (MQ) MAS spectroscopy of rigid solids. The first makes use of ultrafast MAS with spinning frequencies of up to 35 kHz, while the second combines MAS at moderately fast spinning frequencies of about 13 kHz wi
โฆ LIBER โฆ
Resolution Enhancement in Mg NMR Spectroscopy
โ Scribed by Y.Y. Lin; N.H. Ge; L.P. Hwang
- Publisher
- Elsevier Science
- Year
- 1994
- Tongue
- English
- Weight
- 217 KB
- Volume
- 103
- Category
- Article
- ISSN
- 1064-1866
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## Abstract A technique is described which reduced the magnetic susceptibility induced line broadening in NMR spectra obtained from three biological systems at 4.7 Tesla. Proton spectra from a sealed suspension of HL60 leukemic myeioblasts yielded minimum linewidths of 1.3 Hz at 200 MHz (0.0065 ppm