High-Resolution 17O NMR Spectroscopy of Wadsleyite (β-Mg2SiO4).
✍ Scribed by Sharon E. Ashbrook; Andrew J. Berry; William O. Hibberson; Stefan Steuernagel; Stephen Wimperis
- Publisher
- John Wiley and Sons
- Year
- 2003
- Weight
- 55 KB
- Volume
- 34
- Category
- Article
- ISSN
- 0931-7597
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The presence of spinning sidebands can severely compromise pression will not be used, the first criterion is satisfied. the detection of low molarity analytes. Spinning sidebands have Modern NMR spectrometers, appropriately configured, traditionally been minimized by improving the magnetic field hoh
## Abstract Natural abundance solid‐state ^25^Mg NMR measurements were made of the disodium salt of magnesium ethylenediaminetetraacetate tetrahydrate (Na~2~MgEDTA·4H~2~O). Both magic angle spinning (MAS) and static experiments were employed to determine the quadrupole coupling constant (__C__~q~)