✦ LIBER ✦

High-Field High-Speed MAS Resolution Enhancement in 1H NMR Spectroscopy of Solids

✍ Scribed by A Samoson; T Tuherm; Z Gan

Publisher: Elsevier Science
Year: 2001
Tongue: English
Weight: 122 KB
Volume: 20
Category: Article
ISSN: 0926-2040
DOI: 10.1006/snmr.2001.0037

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

High Magnetic Field for Enhanced Proton

High Magnetic Field for Enhanced Proton Resolution in High-Speed CP/MAS Heteronuclear1H–13C Dipolar-Correlation Spectroscopy

✍ B.-J. van Rossum; G.J. Boender; H.J.M. de Groot 📂 Article 📅 1996 🏛 Elsevier Science 🌐 English ⚖ 88 KB

ple-pulse sequences for high-resolution solid-state NMR It is generally accepted that heteronuclear-correlation spectroscopy of biological systems is quite impractical, if spectroscopy in solids requires the application of multiplenot entirely impossible. pulse techniques to achieve sufficient line

Sample-Induced RF Perturbations in High-

Sample-Induced RF Perturbations in High-Field, High-Resolution NMR Spectroscopy

✍ Stuart Crozier; Ian M. Brereton; Fernando O. Zelaya; Wolfgang U. Roffmann; David 📂 Article 📅 1997 🏛 Elsevier Science 🌐 English ⚖ 330 KB

Conducting dielectric samples are often used in high-resolution unwanted signals arising from inaccurate flip angles or other experiments at high field. It is shown that significant amplitude effects. Often phase cycles are used to select particular coand phase distortions of the RF magnetic field m

High-Field and High-Speed CP-MAS13C NMR

High-Field and High-Speed CP-MAS13C NMR Heteronuclear Dipolar-Correlation Spectroscopy of Solids with Frequency-Switched Lee–Goldburg Homonuclear Decoupling

✍ B.-J. van Rossum; H. Förster; H.J.M. de Groot 📂 Article 📅 1997 🏛 Elsevier Science 🌐 English ⚖ 147 KB

On the other hand, the resolution in the upfield region is not In this Communication, we demonstrate that the use of optimal, due to a combination of strong homonuclear dipolar frequency-switched Lee-Goldberg irradiation during the couplings and small shift dispersion for most aliphatic proproton ev

High-resolution 1H NMR spectroscopy of a

High-resolution 1H NMR spectroscopy of absorbed molecules in the presence of strong magnetic fields

✍ J. Roland; D. Michel 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 English ⚖ 136 KB 👁 2 views

Investigation of Templated Mesoporous Si

Investigation of Templated Mesoporous Silicate Thin Films Using High Speed, Solid-State 1H MAS and Double Quantum NMR Spectroscopy

✍ Todd M. Alam; Hongyou Fan 📂 Article 📅 2003 🏛 John Wiley and Sons 🌐 English ⚖ 195 KB

## Abstract Two‐dimensional DQ ^1^H MAS NMR has been used the investigate the local structure of a surfactant‐templated silicate thin film prepared from adding 4% polyoxyethylene(10) cetyl ether to an acidic TEOS silica sol. A close spatial contact between the surfactant and the silicate present in

High-resolution 1H NMR spectroscopy in t

High-resolution 1H NMR spectroscopy in the diagnosis of breast cancer

✍ Silvia Bradamante; Emma Barchiesi; Silvana Pilotti; Giovanni Borasi 📂 Article 📅 1988 🏛 John Wiley and Sons 🌐 English ⚖ 438 KB

Surgical specimens from 22 patients with infiltrating ductal carcinoma of the breast were analyzed by high-resolution 1H NMR spectroscopy at 80 and 300 MHz. Results were compared with those obtained from 9 benign (proliferative dysplasia without atypia) breast samples. NMR spectra at 80 MHz showed w