With capillary electrochromatography CEC performed with capillaries Ε½ packed with octadecylsilica gel, photometric detection in the visible and in the . Ε½ . ultraviolet regions is possible in a packed section in-column detection or an Ε½ . emptied section on-column detection of the separation capilla
Refractive index detection in slurry-packed capillary column LC
β Scribed by Fujimoto, C. ;Morita, T. ;Jinno, K.
- Publisher
- John Wiley and Sons
- Year
- 1986
- Tongue
- English
- Weight
- 338 KB
- Volume
- 9
- Category
- Article
- ISSN
- 0935-6304
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β¦ Synopsis
An existing commercial refractive index detector was modified for use with slurry-packed capillary column LC systems. The cell gasket of the original detector cell was replaced by a micro cell gasket giving a volume of 0.8 pL. The relationship between detector response and the amount of sample injected was examined. The limit of detection was 2-3 ng for di-n-pentyl phthalate.
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