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Reaction of the Boron Halides with the Alkali Metal Hydrides and with Their Addition Compounds; A New Synthesis of Diborane 1

✍ Scribed by Schlesinger, H. I.; Brown, Herbert C.; Gilbreath, James R.; Katz, J. J.

Book ID: 120045607
Publisher: American Chemical Society
Year: 1953
Tongue: English
Weight: 767 KB
Volume: 75
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01097a052

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## Abstract Reduction of 2‐phenyl‐ and 2‐methyl‐__exo__‐3,4‐dichlorobicyclo[3.2.1]oct‐2‐enes with lithium aluminium hydride (LAH) or tributyltin hydride (TBTH) gave __endo__‐2‐phenyl‐3‐chlorobicyclo[3.2.1]oct‐3‐ene, 2‐phenyl‐3‐chlorobicyclo[3.2.1]oct‐2‐ene and their methyl analogues. The action of