## Abstract Radiolabeled forskolin was synthesized by acetylation of deacetylforskolin with ^14^C‐labeled acetic acid in the presence of dicyclohexylcarbodiimide. Separation of labeled forskolin of greater than 97% radiochemical purity was achieved by HPLC with a reversed‐phase column. The synthesi
Rapid synthesis of 2-deoxy-D (1-14C) glucose suitable for labelling with 11C
✍ Scribed by Geneviève Mestelan; Francis Aubert; Jean-Pierre Beaucourt; Dominique Comar; Louis Pichat
- Publisher
- John Wiley and Sons
- Year
- 1979
- Tongue
- French
- Weight
- 327 KB
- Volume
- 16
- Category
- Article
- ISSN
- 0022-2135
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The routine production of 2-deoxy-D-[l-llC] glucose (11C-2DG) 11 from [ C] hydrogen cyanide and 2 , 3 : 4 , 5-di-0-isopropylidene-1-iodo-D-arabinitol is described. The nitrile intermediate is purified by high-performance liquid chromatography (HPLC) before reduction/ hydrolysis with Raney alloy in f
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