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Rapid and efficient procedure for the synthesis of monocyclopentadienyl complexes of hafnium and zirconium

✍ Scribed by Lund, Eric C.; Livinghouse, Tom

Book ID
123611566
Publisher
American Chemical Society
Year
1990
Tongue
English
Weight
253 KB
Volume
9
Category
Article
ISSN
0276-7333

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## The (trimetaphosphimato)hafnates and -zirconates Na 4 {Hf 4 (Β΅ 4 -O)(Β΅-OH) 6 [(PO 2 NH) ), c = 50.284(10) A ˚, Z = 6] were obtained by the stoichiometric reaction of HfOCl 2 β€’ 8 H 2 O and ZrOCl 2 β€’ 8 H 2 O with an aqueous solution of Na 3 (PO 2 NH) 3 β€’ 4 H 2 O, followed by the diffusion-control