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Synthesis of enantiomeric pure zirconium and hafnium benzamidinate complexes

โœ Scribed by Brunner, Tobias S.; Hartenstein, Larissa; Roesky, Peter W.

Book ID
120186855
Publisher
Elsevier Science
Year
2013
Tongue
English
Weight
371 KB
Volume
730
Category
Article
ISSN
0022-328X

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## The (trimetaphosphimato)hafnates and -zirconates Na 4 {Hf 4 (ยต 4 -O)(ยต-OH) 6 [(PO 2 NH) ), c = 50.284(10) A หš, Z = 6] were obtained by the stoichiometric reaction of HfOCl 2 โ€ข 8 H 2 O and ZrOCl 2 โ€ข 8 H 2 O with an aqueous solution of Na 3 (PO 2 NH) 3 โ€ข 4 H 2 O, followed by the diffusion-control