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Pentamethylcyclopentadienyl Zirconium and Hafnium Polyhydride Complexes: Synthesis, Structure, and Reactivity †

✍ Scribed by Visser, Cindy; van den Hende, Johannes R.; Meetsma, Auke; Hessen, Bart; Teuben, Jan H.

Book ID
120159952
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
131 KB
Volume
20
Category
Article
ISSN
0276-7333

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## The (trimetaphosphimato)hafnates and -zirconates Na 4 {Hf 4 (µ 4 -O)(µ-OH) 6 [(PO 2 NH) ), c = 50.284(10) A ˚, Z = 6] were obtained by the stoichiometric reaction of HfOCl 2 • 8 H 2 O and ZrOCl 2 • 8 H 2 O with an aqueous solution of Na 3 (PO 2 NH) 3 • 4 H 2 O, followed by the diffusion-control