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Synthesis, Structure, and Reactivity of C 2 -Symmetric Bis(phospholyl)zirconium and Bis(phospholyl)hafnium Complexes

✍ Scribed by Bellemin-Laponnaz, Stéphane; Lo, Michael M.-C.; Peterson, Thomas H.; Allen, Jerry M.; Fu, Gregory C.

Book ID
127054244
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
87 KB
Volume
20
Category
Article
ISSN
0276-7333

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The reaction of 2,3,4,5-tetramethylphospholylpotassium alkyl complexes [(C 4 Me 4 P) 2 LnCH(SiMe 3 ) 2 ]; these complexes were most efficiently prepared from [LnCl 3 (THF) x ], [C 4 Me 4 PK] with [LnCl 3 (THF) x ] (Ln = Nd, Sm) in a 2:1 ratio gave unsolvated ate complexes of the formula [KC 4 Me 4 P